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Fluoroquinolone Antibiotics in Beef Kidney - Tandem Oasis MAX-MCX Method

Fluoroquinolone Antibiotics in Beef Kidney - Tandem Oasis MAX-MCX Method

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Beef kidneys with Madeira sauce

This is an Application Brief and does not contain a detailed Experimental section.

Abstract

This application brief demonstrates analysis of fluoroquinolone antibiotics in beef kidney - Tandem Oasis MAX-MCX method.

Introduction

The compounds used in this study are - Ciprofloxacin and Enrofloxacin.

Experimental

Mobile phase Conditions

Column:

Atlantis dC₁₈ 4.6 x 150 mm, 5 μm

Mobile phase:

73% 0.2% NFPA (nonafluoropentanoic acid)

4% MeOH

23% ACN

T=30

Results and Discussion

HPLC Chromatogram of Fluoroquinolone Antibiotics in Beek Kidney by Single Cartridge Extraction

HPLC Chromatogram of Fluoroquinolone Antibiotics in Beek Kidney by Tandem Oasis MAX/MCX Extraction

Conclusion

Comparison of results of Tandem Oasis MAX-MCX vs. Single Cartridge was carried out.

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WA31764.86, June 2003