This is an Application Brief and does not contain a detailed Experimental section.
This application brief demonstrates the analysis of doxepin in serum using Symmetry Columns.
The compounds analyzed in this study are:
 
            
        | Column: | Symmetry Shield RP8, 3.9 x 150 mm, 5 µm | 
| Guard Column: | Symmetry Guard Column, 3.9 x 20 mm, 5 µm | 
| Part numbers: | Column - WAT200655, Guard - WAT200675 | 
| Mobile phase: | 20 mM potassium phosphate, pH 7/methanol 38:62 | 
| Flow rate: | 1.0 mL/min | 
| Injection volume: | 20 µL of reconstituted porcine serum extract | 
| Temperature: | 30 °C | 
| Detection: | UV @ 254 nm | 
 
            
         
            
         
            
        WA31763.79, June 2003