Mass Spectrometry (XEVO TQ) standards kit for system assessment. 10 Components
1. 1X 25mL Tuning Solution X 10: Acetominophen (4-Acetamidophenol) 200pg/ul, Caffeine 200pg/ul, Sulfadimethoxine 100pg/ul, Verapamil, 50pg/ul, Chloramphenicol, 50pg/ul, 1 x 17-A-Hydroxyprogesterone, 5000pg/ul in 90% MeOH:10% Water Flame Sealed Ampule
2. 1 x 30mL Set up Solution QP: PPG1000 2.5 ng/ul, Triacetyl-B-cyclodextrin 5.0 ng/ul, Verapmil 100.0 pg/ul, Leucine Enkaphalin 1.0 ng/ul, Ammonium Acetate 0.31 mg/ml Acetonitrile/Water (1:1 V/V) Clear Nalgene Bottle
3. 1 x 30mL Calibration Solution: Sodium Iodide 2 ug/ul (+1%, -0%) Cesium Iodide 50 ng/ul (+1%, -0%) IPA/Water (1:1 V/V), Clear Nalgene Bottle 4. 1X 10mg Ion Sabre APCI Pos Sensitivity: 17-alphahydroxyprogesterone 10 mg solid in 4 ml Amber Screw Top Vial 5. 1X 50 mg ESI Negative Sensitivity: Chloramphenicol Solid 50mg 8 ml Amber Screw Top Vial
6. 1 X 5mg ESI Positive Sensitivity: Reserpine solid 5 mg in 4 ml Amber Screw Top Vial
7. 1 x 5mg Ion Sabre APCI Neg Sensitivity: Sulfadimethoxine Solid 5mg in 4 ml Amber Screw Top Vial
8. 1 x 0.1mg*Scanwave optimisation: [Glu1]-Fibrinopeptide B 0.1 mg ±0.01 mg in 4 mL Amber Screw top Vial
9. 1 x 3mL Mobile phase additiveAqueous Ammonia Specific Gravity - 0.88 to 0.89 (~30% w/w ammonia) Flame sealed ampule
10. 2 x 1mL Mobile phase additive: Formic Acid 98-100% Purity Flame sealed ampule
1 X 715001937 Solution Prep – Xevo TQ Document
1 Clear Nalgene Bottle 30ml
Certificate of Analysis
