Demonstration of LC-MS Nitrosamine Impurity Quantification Performance using Automated Sample Preparation with the Andrew+ Pipetting Robot

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Mary Trudeau, Nigel Skinner
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Application Notes
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This automated method created with OneLab, and performed on the Andrew+ Pipetting Robot, developed herein, was able to perform simple serial dilution to generate calibration curves for analysis of nitrosamine impurities with no manual intervention by the analyst. This broadly applicable method can be use independently, or as part of a more complex sample workflow for robust LC-MS quantification analysis. In addition, OneLab methods are traceable and easily transferable, ensuring method reproducibility performance: day-to-day, user-to-user, system-to-system, and lab-to-lab.

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