Routine UPLC-MS/MS Quantification of Pesticide Residues in Okra with Simultaneous Acquisition of Qualitative Full-Spectrum MS and MS/MS Data

Library Number:
APNT134765520
Part Number:
720004789EN
Author(s):
Dimple Shah, Mark Benvenuti, Antonietta Gledhill, P. M. N. Rajesh, and Jennifer A. Burgess
Source:
Waters
Content Type:
Application Notes
Content Subtype:
Application Notes
Related Products:
 
 
 
 
 

In this application note, a multi-residue analysis method for the detection of 212 pesticides in okra is presented.

The combination of ACQUITY UPLC H-Class System with the Xevo TQD tandem mass spectrometer can detect pesticides below the legislative limit in okra samples.  Even though a strong matrix effect was observed for many compounds, detection and quantification at the legislative limit was achieved. Simultaneous acquisition of MRMs and RADAR full-scan data provides quantitative and qualitative information in single injection.  Product ion confirmation (PICs) increases confidence in compound assignments, which proves highly useful when working with complex matrices.


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